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M."F."BRAÑA"y"col."
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Tabla'1.'7!Características!de!las!N5(45piridilmetil)benzamidas.!
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COM. R. MET. CRYST. P.F. ºC Rto.% REF.
1H B EtOH/H20 114-5 60 14
2 4-CH3 B H20 130-1 70 13
104-5 65 ---
3 3-CH3 B DMF/H20 146-8 50 13
4 2-CH3 B DMFH20 127-0 90 ---
5 4-t-C4H9 B BENCENE 138-0 65 13
6 4-OCH3 B H20 150-2 70 ---
>260 40 13
7 4-SCH3 B EtOH/H20 198-0 66 ---
8 4-0H B DMF/H20 260 86 13
206-7 61 ---
9 4-NO2 A EtOH/H20 233-5 67 ---
235-7 65 ---
10 4-NH2 9+H2/Pd DMF/H20 193-4 69 ---
133-4 64 13
11 4-N(CH3)2 B DMF/H20 88-0 53 ---
98-9 50 12
12 4-NHCOCH3 B H20 144-6 58 ---
88-0 30 13
13 4-SO2NH2 B H20 167-9 94 12
14 4-C6H5 B MeOH/H20 180-1 42 ---
15 4-Cl B DMF/H20
16 3-Cl B EtOH/H20
17 2-Cl B EtOH/H20
18 3,5-Cl2 B DMF/H20
19 4-F A AcOEt/He
20 4-CF3 C MeOH
21 4-NHSO2C6H5 B AcOEt
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